The method is suitable for the determination of water vapor volatile aroma compounds in beer.
Volatile aroma compounds are driven out of the sample through steam distillation. The ethanolic distillate is saturated with NaCl. Potassium hydrogen sulfite is added to separate carbonyl groups that might interfere with the analysis. The extraction of the aroma compounds is performed by shaking out with dichloromethane and the phases separated by centrifuging.
Hops and hop products intended for use in beer brewing or elsewhere in the food industry
A reliable sampling method for whole hops and hop products is a prerequisite for obtaining suitable material for analysis. The effort involved in collecting the sample depends upon how uniform the hop product is.
Determination of xanthohumol and isoxanthohumol
All beers, beer-based beverages, wort, ethanol extracts, CO2 spent hops and xanthohumol products
Xanthohumol and isoxanthohumol are dissolved with acetonitrile from the sample and following separation, are determined using a Nucleodur C18 column and UV detection.
This method describes the determination of four hop aroma compounds found in hops and hop products using gas chromatography.
Hops and hop products intended for use in beer brewing or elsewhere in the food industry
The hop oil obtained through steam distillation (refer to links) is dissolved in an organic solvent, separated into its components by means of gas chromatography and determined with a flame ionization detector. The contents are expressed as a percentage of the area of each component compared to the overall area of the peak.
Whole hops intended for use in beer brewing or elsewhere in the food industry
Evaluation of the appearance of hop cones is performed through visual inspection and sensory assessment.
This method describes how to correctly collect a sample of water.
Water intended for use as an ingredient in the production of beer (brewing liquor) or other foods
Collecting samples correctly is a prerequisite for obtaining flawless analytical results. The sample collection method must be adapted to align with the purpose of the analysis method. As a rule, separate samples are taken for chemical and microbiological analyses, since different equipment and containers are required for the collection and treatment of samples.
In principle, sample collection methods are distinguished as follows:
Random samples collected for analysis identify possible contamination or can be collected for purposes of orientation prior to more extensive sampling.
Both intermittent (discontinuous) sample collection (according to certain time intervals, volumes or flow rates) and continuous sampling, which allows for constant monitoring of flowing water for compliance with quality standards, are possible. Samples taken continuously can be mixed to create composite samples and provide mean data.
A series of samples (taken at different depths or over a given area to perform profile tests) are collected for analysis in the process of testing standing water.