Determination of the aluminum content in beer
This method is suitable for beer.
The aluminum in beer is measured using the flameless AAS technique; the measurement is performed at 309.3 nm.
Determination of the concentration of alkaline cleaners in sodium hydroxide (NaOH) and aluminum (Al).
All alkaline cleaning solutions or "stack solutions" that contain dissolved aluminum (Al3+) and/or soda (Na2CO3) in addition to sodium hydroxide (NaOH) as a cleaning component.
The sodium hydroxide bound as aluminate and titrated in the p-value determination is calculated by subsequent determination of the aluminum and deducted, as it is no longer available for purification.
The aluminum determination itself is based on the reaction between aluminum hydroxide and sodium fluoride, in which sodium hydroxide is released and thus serves as a measure for calculating the aluminum.
Carbonates interfering with the titration are precipitated with Ba2+ ions.
This method describes the determination of aluminum in wort or Congress wort by means of atomic absorption spectrometry.
Suitable for analysis of all (laboratory) wort samples
Aluminum in wort is measured using the flameless AAS technique; the measurement is made at 309.3 nm.
The cations in beer and wort are determined with this analysis.
This method is suitable for both wort and beer.
Inductively coupled plasma optical emission spectroscopy (ICP-OES) is a fast and reliable method for the laboratory analysis of metals. Inductively coupled plasma (ICP), a high frequency field of ionized gas, serves as a medium for atomizing and exciting the substances found in samples. Liquid, dissolved or aerosol samples are injected into the ionized gas stream. In emission spectroscopy, ICP can be used in conjunction with a number of optical and electronic systems either simultaneously or sequentially in multi-element spectrometers. In the plasma, the atoms and ions are excited to a higher energy state bringing about the emission of electromagnetic radiation (light), primarily in the ultraviolet and visible region of the spectrum. Metals ordinarily occur as ions in the temperature range typical for ICP of 6000 to 10000 K; however, non-metals and metalloids are only partially ionized.
ICP-OES operates within a very wide range. This usually encompasses six orders of magnitude in concentrations smaller than μg/l up to g/l, depending upon the element and the concentrations used for the set of analysis data. With ICP-OES, beer and wort can also be analyzed without prior processing of the samples, in contrast to AAS. Methods for determining the following in beer and wort will be described below: Al, B, Ba, Ca, Co, Cu, Fe, K, Mg, Mn, Mo, Na, P, Si, Sr, Sn and Zn.
Water intended for use as an ingredient in the production of beer (brewing liquor) or other foods
Oils and fats dispersed in water are precipitated using aluminum sulfate. After dissolving the precipitate with hydrochloric acid in organic solvents, they can be separated from the mineral salts.
All alkaline cleaning solutions or "stack solutions" that contain sodium hydroxide (NaOH) as well as dissolved aluminum and/or soda (Na2CO3) in addition to free chlorine.
Alkaline cleaning agents and disinfectants containing chlorine can be determined by their alkalinity concentration. The chlorine present destroys most indicators by oxidation. Before adding the indicator, the chlorine must be eliminated by adding sodium thiosulphate to the sample.