Determination of the concentration of dissolved carbon dioxide in carbonated beverages by means of volumetric expansion
This analysis is suitable for determining the concentration of dissolved carbon dioxide in carbonated beverages by means of volumetric expansion at concentrations between 2.5 and 6.2 g/l.
This device makes use of a method patented and entitled by Anton Paar "Multiple Volume Expansion". Here, the volume in the measuring chamber is increased in two separate steps, and at the end of each step the equilibrium pressure and temperature are recorded for use in the calculation. The true carbon dioxide content is determined independently of any other gases which may be dissolved in the beverage [1, 2, 3].
The figure below depicts the calibration correcting for air in the sample and shows how the effect of any dissolved gases other than CO2 (air or nitrogen) on the result of the analysis is eliminated using the volumetric expansion employed in this method. The CO2 content is determined after two separate volumetric expansions in the measuring chamber. If no dissolved other gases are present in the sample, the two results are identical, and no correction is necessary. If gases other than CO2 are dissolved in the sample, this causes the result to be lower after the larger volumetric expansion (the second measurement) than the result at smaller volumetric expansion (the first measurement). A correction value is calculated based upon the difference between the two results, which completely eliminates the influence of the dissolved foreign gases (air or nitrogen) on the ultimate result of the analysis.
This method describes how to determine the hectoliter weight of barley.
Barley intended for the production of malt is evaluated on the basis of the hectoliter weight.
The hectoliter weight determines how many kilograms 100 liters of barley weighs. For this analysis, the weight of a defined sample volume of barley is determined, and the corresponding hectoliter weight is calculated.
One hectoliter of malting barley generally weighs between 68 and 75 kg, although higher values are not unusual (up to 78 kg).
This method describes how to determine the hectoliter weight of malt.
Barley malt intended for use in beer brewing or elsewhere in the food industry.
The hectoliter weight determines how many kilograms 100 liters of malt weighs. This analysis provides an estimate for the volumetric space required for storage and transport of a lot of malt.
Determination of the "air volume" (gas volume other than carbon dioxide) in the headspace of bottles and cans
Suitable for determination in beer, mixed beer beverages and carbonated beverages
The method provides valuable information on effective and uniform foaming and undercap gassing during can filling.
The gas in the headspace of bottles and cans is captured under a funnel filled with water and subsequently migrates very slowly through a column of liquid containing potassium hydroxide or sodium hydroxide, whereupon the carbon dioxide also contained in the headspace is bound by the caustic solution. The remaining gas, consisting of nitrogen and oxygen, is captured in a burette, from which the volume can be read. The value from the burette is expressed as “air in headspace” [1].
Determination of the "air volume" (gas volume other than carbon dioxide) and oxygen in the headspace of cylinders and cans
Suitable for determination in beer, mixed beer beverages and carbonated beverages
The burette containing the caustic solution, in this case, is equipped with a short capillary outlet. A tube is attached to this outlet, connecting the burette to a second burette with a lower capillary outlet. The second burette contains an alkaline solution of sodium dithionite, which binds oxygen [1, 2]. In the first burette, the volume of air is measured, and in the second, the volume of nitrogen.