B-400.28.33 [2020-10] Vitamins B1 and B2 – HPLC

Barley and malt are rich in vitamins and are localized in the living tissues of the embryo and of the aleurone layer. They are involved in building enzymes as part of a prosthetic group. Of the vitamins in the B complex, vitamin B1 is present in barley in amounts ranging from 1.2–7.4 mg/kg barley, dry matter. During germination, the concentration of vitamin B2 increases to 1.5 times the quantity found in barley. This corresponds to a concentration of 1–3.7 mg/kg malt, dry matter.

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Application/Purpose

Determination of vitamin B1 (thiamine) and B2 (riboflavin) in mash, wort and beer

Scope of Application

Suitable for all types of wort and beer

Principle

HPLC methods have been successfully used for the analysis of vitamin content in non-alcoholic beverages. However, for the most part, these methods cannot be employed with a wort or beer matrix due to the vitamin concentrations present.

The reagent kit for the determination of vitamins B1 and B2 in blood from Chromsystems GmbH in Munich, Germany was used for the analysis. This company specializes in the manufacture of reagent kits for clinical applications. The kits are easy to use and do not require much additional equipment; a simple isocratic HPLC system is sufficient. In cooperation with the company, this kit was modified to accommodate a different sample matrix (mash, wort and beer).

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